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Comparative study of commercial cold-cuts used NIRS and sensory analysis

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Comparative study of commercial cold- cuts used NIRS and sensory analysis

Judit Belovai , R. Romvári, Gy. Bázár, A. Szabó

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Introduction

• Improvement of the nutritional science and the health-sound behaviour of consumers

• Sensory and chemical characterization of heat-treated meat products

• Sensory properties have primary importance from the aspect of consumer perception

• BUT: The ingredients are also highlight of food

• Healthy nutrition is a spreading trend

• Improvement of the nutritional science and the health-sound behaviour of consumers

• Sensory and chemical characterization of heat-treated meat products

• Sensory properties have primary importance from the aspect of consumer perception

• BUT: The ingredients are also highlight of food

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Introduction

• Sensory analysis :

Answer important questions during processing

Help to elucidate production faults, to monitor the quality

Help to compare production lots or differently developed products

• Need the chemical composition as well  near infrared spectroscopy  used widely in the food industry:

Minimal sample preparation

Give multitude information from a single spectrum

Quantitative and qualitative analysis

Estimation methods

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The Purpose

This study aimed to classify commercial cold-cut

sorts (Lyoner samples of different quality and

price), based on sensory tests and NIR

spectroscopy.

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Materials and methods

Material

NIR spectroscopy

FOSS NIRSystems 6500 spectrometer equipped with:

WinISI II v1.5 spectral analytical software

Sensory analysis

Full profile analysis (MSZ ISO 6564:2001)

13 university students and teachers

10 cm long, unstructured scale

SPSS 10.0. for Windows

PanelCheck V.1.3.2. statistical softwares

sample code price HUF/kg 1 1188 (cca. 4 Euro/kg) 2 941 (cca. 3 Euro/kg) 3 941 (cca. 3 Euro/kg) 4 710 (cca. 2.5 Euro/kg) 5 1878 (cca. 6 Euro /kg)

Regular Sample Transport Module (STM) OptiProbe fiber optic

module

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Results and

discussion

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Results of the Panel Check

Character of taste Spiciness Taste acception Character of odour Oduor acception Texture elasticity Air and gel bubbles Homogenity Texture acception Colour intensity Colour acception General Impression Character of taste Spiciness Taste acception Character of odour Oduor acception Texture elasticity Air and gel bubbles Homogenity Texture acception Colour intensity Colour acception General Impression

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PCA analysis of Sensory results

Air and gel bubbles

Homogenity

General Impression Oduor acception

Texture acception

Taste acception

Colour acception

Colour intensity

(~4 euro)

(~3 euro)

(~3 euro)

(~2,5 euro)

(~6 euro)

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DFA analysis of Sensory results

Group 1 2 3 4 5

Classification

1 81,8 0 0 0 18,2

2 9,1 63,6 9,1 18,2 0

3 0 9,1 81,8 0 9,1

4 0 9,1 9,1 81,8 0

5 18,2 0 0 9,1 72,7

Cross- validation

1 72,7 9,1 9,1 0 9,1

2 9,1 36,4 36,4 9,1 9,1

3 9,1 36,4 36,4 9,1 9,1

4 9,1 9,1 18,2 45,5 18,2

5 18,2 0 9,1 18,2 54,5

Classification: 76.3%

Cross-validation: 49.1%

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Near Infrared Spectroscopy

0.049 5.374

STM Optiprobe

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PCA analysis of Near Infrared Spectroscopy results

STM

1 2 3

4 5

Optiprobe

2 3 14

5

(~3 euro) (~3 euro)

(~6 euro) (~2,5 euro) (~4 euro)

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Comparative table of the methods

PCA DFA

(Cross-validation)

NIRS - STM 94% 98%

NIRS - Optiprobe 85% 71%

Sensory analysis n.d. 49,1%

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Summary

• Based on the human panel test, the cold-cut sorts of lower quality and price provide compromised homogenity.

• In connection with this, panellists found air sacs and gel bubbles in these samples.

• The preference was markedly higher by samples of higher price- niveau, mostly attributed to the “overall impression” and

“preference” characteristics.

• As compared to the discriminant factor analysis based on the sensory panel test, the NIR based classification was more successful.

• Latter method can be adapted to industrial processes even in an on- line manner, and provides a low-cost analytical possibility at high sample numbers.

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