• Nem Talált Eredményt

ADDITIONAL INFORMATION FOR CHAPTER 8

Figures 116 and 117 show two other sizes of digestion flasks sometimes used, namely the 1 0 -

5

>

1 9 3

>

1 9 4

and 1 0 0 -

1 9 3

>

1 9 4

m l . sizes.

2 1 0 + 5 MM

2 1 . 5 _ o rBEAD A n

MM M A X .

APPROX. I SQ CM SANDBLASTED , AREA (FOR L A B E L L I N G )

2 0 ± 0 . 5 MM O.D.

WALL 1.0-1.5 MM

FIG. 117. Kjeldahl digestion flask, 100 ml.—details of construction.

T A B L E 19

ADDITIONAL INFORMATION ON R E F E R E N C E S * RELATED TO C H A P T E R 8

In addition to the procedures described in detail in the preceding pages of this chapter, the author wishes to call to the attention of the reader many of the investiga­

tions in connection with the microdetermination of nitrogen by the Kjeldahl method. These are listed in Table 19 and the same plan is used here as was used in the preceding chapters. (See statement at top of Table 4 of Chapter 1, regarding completeness of this material.)

Books Collaborative studies

Association of Official Agricultural Acree, 1

Chemists, 6 Clark, 40

Belcher and Godbert, 21, 22 Lake, 107

Clark, E . P., 41 Ogg, 142, 143

Clark, S. J . , 42 Ogg and Willits, 145, 146

Furman, 66 Willits and Ogg, 2 1 6 - 2 2 0

Grant, 73, 74

Kirk, 98

Without microchemical balance

Milton and Waters, 130, 131 Niederl and McBeth, 136 Niederl and Niederl, 137, 138

Niederl and Sozzi, 1 3 9

Apparatus

Pregl, 157 Asami, 7

Roth, 1 6 3 - 1 6 6 Ballentine and Gregg, 10

Steyermark, 1 9 3 Berck, 24

General, miscellaneous, reviews

Brant and Sievers, 34, 35

General, miscellaneous, reviews

British Standards Institution, 37

American Instrument Company, 4 Clark, E. P., 40, 41

Bode, 26 Doherty and Ogg, 53

Bradstreet, 31 Eder, 55

Dittrich and deVries, 51 Furman, 66

Gomez Vigide, 70 Grant, 73, 74

Gonzalez Carrero, Carballido Ramallo, Hallett, 78

and Gomez Vigide, 7 1 , 72 Jenden and Taylor, 89

Hirai and Hayatsu, 85 Johanson, 90

Hu, 86 Kemmerer and Hallett, 9 3

Kainz, 9 1 Kirk, 9 6- 9 8

Kirk, 95, 98 Kirsten, 99

Levin, Oberholzer, and Whitehead, 112 Klingmuller, 101 Machemer and McNabb, 118 Leurquin and Delville, 111 McKenzie, Wake and Wallace, 124 Machemer and McNabb, 118 Rush, Cruikshank, and Rhodes, 167 Marino, 120

Schulek, Burger, and Fehér, 174 Miller, 126

Stegemann, 190 Mohlau, 132, 133

Stetten, 191 Niederl and Niederl, 137, 138

White and Secor, 211 Nogrâdy, 141

White, Secor, and Long, 212 Parnas, 149 Wingo, Davis, and Anderson, 222 Parnas, 150

* The numbers which appear after each entry in this table refer to the literature citations in the reference list at the end of the chapter.

T A B L E 19 (Continued)

Grunbaum, Kirk, Green, and Koch, 75 Grunbaum, Schaffer and Kirk, 76

T A B L E 19 (Continued)

Grunbaum, Kirk, Green, and Koch, 75 Kirsten, 100

Secor, Long, Kilpatrick, and White, 179 Willits and Ogg, 218, 219

T A B L E 19 (Continued) Spectrophotometry, colorimetric, Other methods

chromatographic, etc., methods Dumas, see Chapter 7 Hussey and Maurer, 87

Milner, Zahner, Hepner, and Cowell, 129 Scheurer and Smith, 171

2. Acculate, Anachemia Chemicals, Ltd., Montreal, Quebec, and Champlain, New York.

3. Adams, C. L, and Spaulding, G. H., Anal. Chem., 27, 1003 ( 1 9 5 5 ) .

4. American Instrument Co., Inc., "Digestion and Distillation Apparatus for the Micro Kjeldahl Nitrogen Determination," Bull. No. 2271, Silver Springs, Mary­

land, 1955.

5. American Society for Testing Materials, AST M Designation, Ε 147-59 Τ ( 1 9 5 9 ) . 6. Association of Official Agricultural Chemists, "Official Methods of Analysis," 8th

ed., pp. 8 0 1 - 8 1 1 , Washington, D . C , 1955.

19. Belcher, R., and Bhatty, M. K., Mikrochim. Acta, p. 1183, 1956.

20. Belcher, R., and Godbert, A. L., / . Soc. Chem. Ind. (London), 60, 196 ( 1 9 4 1 ) . 21. Belcher, R., and Godbert, A. L., "Semi-Micro Quantitative Organic Analysis,"

Longmans, Green, London, New York, and Toronto, 1945.

22. Belcher, R., and Godbert, A. L., "Semi-Micro Quantitative Organic Analysis," 2nd ed., Longmans, Green, London, 1954.

30. Bradstreet, R. B., Anal. Chem., 32, 114 ( i 9 6 0 ) . 38. Briiel, D., and Holter, H., Compt. rend. trav. lab. Carlsberg. Sér. chim., 25, 289

( 1 9 4 7 ) .

39. Cepciansky, I., and Chromcova, L., Chem. prûmysl, 9, 188 ( 1 9 5 9 ) ; Anal. Abstr., 6, No. 4802 ( 1 9 5 9 ) .

40. Clark, E. P., / . Assoc. Offic. Agr. Chemists, 24, 641 ( 1 9 4 l ) .

41. Clark, E. P., "Semimicro Quantitative Organic Analysis," Academic Press, New York, 1943.

42. Clark, S. J . , "Quantitative Methods of Organic Microanalysis," Butterworths, London, 1956.

43. Cole, J . O., and Parks, C. R., Ind. Eng. Chem., Anal. Ed., 18, 61 ( 1 9 4 6 ) . 44. Dalrymple, R. S., and King, G. B., Ind. Eng. Chem., Anal. Ed., 17, 403 ( 1 9 4 5 ) . 45. Day, H. G., Bernstorf, E., and Hill, R. T., Anal. Chem., 21, 1290 ( 1 9 4 9 ) .

46. Dermelj, M., and Strauch, L., Bull. sci. Conseil acad. RPF Yougoslavie, 3, 6 ( 1 9 5 6 ) .

66. Furman, Ν. H., ed., "Scott's Standard Methods of Chemical Analysis," 5th ed., Vol. II, Van Nostrand, New York, 1939.

67. Furter, M. F., Personal communication.

68. Gaberman, V., Voprosy Med. Khim., 3, 464 ( 1 9 5 7 ) ; Chem. Abstr., 52, 12663 ( 1 9 5 8 ) .

69. Gardon, J . L., and Leopold, B., Anal. Chem., 30, 2057 ( 1 9 5 8 ) .

70. Gomez Vigide, R. F., Inform, qutm. anal. (Madrid), 12, 9 ( 1 9 5 8 ) ; Anal. Abstr., 5, No. 3767 ( 1 9 5 8 ) .

71. Gonzalez Carrero, J . , Carballido Ramallo, O., and Gomez Vigide, F., Inform.

quim. anal. (Madrid), 10, 199 ( 1 9 5 6 ) .

72. Gonzalez Carrero, J . , Carbillado Ramallo, O., and Gomez Vigide, F., Proc. Intern.

Cong. Pure and Appl. Chem., Anal. Chem. 15th Congr., Lisbon, 1, 101 ( 1 9 5 6 ) ; Anal. Abstr., 6, No. 1175 ( 1 9 5 9 ) .

73. Grant, J . , "Quantitative Organic Microanalysis, Based on the Methods of Fritz Pregl," 4th ed., Blakiston, Philadelphia, Pennsylvania, 1946.

74. Grant, J . , "Quantitative Organic Microanalysis," 5th ed., Blakiston, Philadelphia, Pennsylvania, 1951.

98. Kirk, P. L., "Quantitative Ultramicroanalysis," Wiley, New York, and Chapman

& Hall, London, 1 9 5 0 ; "The Chemical Determination of Proteins," in "Ad­

vances in Protein Chemistry" ( M . L. Anson, and J . T . Edsall, eds.), Vol. 3,

109. Lauro, M. F., Ind. Eng. Chem., Anal. Ed., 3, 401 ( 1 9 3 1 ) .

124. McKenzie, Η. Α., Wake, R. G., and Wallace, H. S., Proc. Intern. Congr. Pure and Appt. Chem., Anal. Chem. 15th Congr., Lisbon 1 ( 1 9 5 6 ) ; Anal. Abstr., 6, No.

130. Milton, R. F., and Waters, W . Α., "Methods of Quantitative Microanalysis,"

Longmans, Green, New York, and Arnold, London, 1949.

131. Milton, R. F., and Waters, W . Α., "Methods of Quantitative Microanalysis," 2nd ed., Arnold, London, 1955.

137. Niederl, J . B . , and Niederl, V., "Micromethods of Quantitative Organic Elementary Analysis," Wiley, New York, 1938.

138. Niederl, J . B . , and Niederl, V., "Micromethods of Quantitative Organic Analysis,"

2nd ed., Wiley, New York, 1942.

139. Niederl, J . B . , and Sozzi, J . Α., "Microanâlisis Elemental Orgânico," Calle Arcos, Buenos Aires, 1958.

149. Parnas, J . Κ., Z. anal. Chem., 114, 261 ( 1 9 3 8 ) .

157. Pregl, F., "Quantitative Organic Microanalysis," ( E . Fyleman, trans., 2nd German ed.), Churchill, London, 1924.

158. Rappaport, F., Mikrochemie, 14, 49 ( 1 9 3 3 ) .

159. Rauen, H. M., and Buchka, M., Angew. Chem., 60A, 209 ( 1 9 4 8 ) .

160. Ribas, I., and Lopez Capont, F., Anales real soc. es pan. fis. y quim. (Madrid), 4 6 B , 581 ( 1 9 5 0 ) .

161. Ribas, I., and Vâsquez-Gesto, D., Inform, quim. anal. (Madrid), 7, 29 ( 1 9 5 3 ) . 162. Roth, H., Mikrochemie ver. Mikrochim. Acta, 31, 287 ( 1 9 4 4 ) .

163. Roth, H., "Die quantitative organische Mikroanalyse von Fritz Pregl," 4th ed., Springer, Berlin, 1935.

164. Roth, H., " F . Pregl quantitative organische Mikroanalyse," 5th ed., Springer, Wien, 1947.

165. Roth, H., "Pregl-Roth quantitative organische Mikroanalyse," 7th ed., Springer, Wien, 1958.

166. Roth, H., "Quantitative Organic Microanalysis of Fritz Pregl," 3rd ed. ( Ε . B . Daw, trans., 4th German ed.), Blakiston, Philadelphia, Pennsylvania, 1937.

167. Rush, C. Α., Cruikshank, S. S., and Rhodes, E. J . H., Mikrochim. Acta, p. 858 178. Scientific Glass Apparatus Company, Bloomfield, New Jersey.

179. Secor, G. E., Long, M. C , Kilpatrick, M. D., and White, L. M., / . Assoc. Offic.

189. Sobel, A. E., Mayer, A. M., and Gottfried, S. P., / . Biol. Chem., 156, 355 ( 1 9 4 4 ) . 190. Stegemann, H., Z. physiol. Chem., 312, 255 ( 1 9 5 8 ) .

191. Stetten, D., Jr., Anal. Chem., 23, 1177 ( 1 9 5 1 ) . 192. Steyermark, Al, Unpublished work.

193. Steyermark, Al, "Quantitative Organic Microanalysis," Blakiston, Philadelphia, Pennsylvania, 1951. 198. Swedish Iron & Steel Corp., Westfield, New Jersey.

199- Takeda, Α., and Senda, J . , Ber. Ôhara Inst, landwirtsch. Biol., Okayama Univ., 10, 241 ( 1 9 5 6 ) .

200. Taylor, W . H., and Smith, G. F., Ind. Eng. Chem., Anal. Ed., 14, 437 ( 1 9 4 2 ) . 201. Terent'ev, A. P., and Luskina, Β . M., Zhur. Anal. Khim., 14, 112 ( 1 9 5 9 ) . 202. Thomas, Arthur H., Company, Philadelphia, Pennsylvania.

203. Thompson, J . F., and Morrison, G. R., Anal. Chem., 23, 1153 ( 1 9 5 1 ) . 221. Willits, C. O., and Ogg, C. L., Personal communication.

222. Wingo, W . J . , Davis, O. L., and Anderson, L , Anal. Chem., 22, 1340 ( 1 9 5 0 ) . 223. Wust, H., Klin. Wochschr., 32, 27, 660 ( 1 9 5 4 ) .

224. Zakrzewski, Z., and Fuchs, H. J . , Biochem. Z., 285, 390 ( 1 9 3 6 ) . 225. Zinneke, F., Angew. Chem., 64, 220 ( 1 9 5 2 ) .