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Article

Parametric Effects of Single Point Incremental Forming on Hardness of AA1100 Aluminium Alloy Sheets

Sherwan Mohammed Najm1,2,* , Imre Paniti1,3 , Tomasz Trzepieci ´nski4 , Sami Ali Nama5, Zsolt János Viharos3,6and Adam Jacso1

Citation: Najm, S.M.; Paniti, I.;

Trzepieci ´nski, T.; Nama, S.A.; Viharos, Z.J.; Jacso, A. Parametric Effects of Single Point Incremental Forming on Hardness of AA1100 Aluminium Alloy Sheets.Materials2021,14, 7263.

https://doi.org/10.3390/ma14237263

Academic Editors: Jie Zhou and Valentin ¸Stefan Oleksik

Received: 14 October 2021 Accepted: 17 November 2021 Published: 27 November 2021

Publisher’s Note:MDPI stays neutral with regard to jurisdictional claims in published maps and institutional affil- iations.

Copyright: © 2021 by the authors.

Licensee MDPI, Basel, Switzerland.

This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://

creativecommons.org/licenses/by/

4.0/).

1 Department of Manufacturing Science and Engineering, Budapest University of Technology and Economics, M ˝uegyetem rkp 3, H-1111 Budapest, Hungary; imre.paniti@sztaki.hu (I.P.); jacso.adam@gpk.bme.hu (A.J.)

2 Kirkuk Technical Institute, Northern Technical University, Kirkuk 41001, Iraq

3 Centre of Excellence in Production Informatics and Control, Institute for Computer Science and Control (SZTAKI), Kende u. 13-17, H-1111 Budapest, Hungary; viharos.zsolt@sztaki.hu

4 Department of Manufacturing and Production Engineering, Faculty of Mechanical Engineering and Aeronautics, Rzeszow University of Technology, Al. Powst. Warszawy 8, 35-959 Rzeszów, Poland;

tomtrz@prz.edu.pl

5 Engineering Technical College, Middle Technical University, Baghdad 10074, Iraq; drsami@mtu.edu.iq

6 Department of Management and Business Law, Faculty of Economics and Business, John von Neumann University, Izsáki Str. 10, H-6000 Kecskemét, Hungary

* Correspondence: sherwan.mohammed@gpk.bme.hu

Abstract:When using a unique tool with different controlled path strategies in the absence of a punch and die, the local plastic deformation of a sheet is called Single Point Incremental Forming (SPIF). The lack of available knowledge regarding SPIF parameters and their effects on components has made the industry reluctant to embrace this technology. To make SPIF a significant industrial application and to convince the industry to use this technology, it is important to study mechanical properties and effective parameters prior to and after the forming process. Moreover, in order to produce a SPIF component with sufficient quality without defects, optimal process parameters should be selected.

In this context, this paper offers insight into the effects of the forming tool diameter, coolant type, tool speed, and feed rates on the hardness of AA1100 aluminium alloy sheet material. Based on the research parameters, different regression equations were generated to calculate hardness. As opposed to the experimental approach, regression equations enable researchers to estimate hardness values relatively quickly and in a practicable way. The Relative Importance (RI) of SPIF parameters for expected hardness, determined with the partitioning weight method of an Artificial Neural Network (ANN), is also presented in the study. The analysis of the test results showed that hardness noticeably increased when tool speed increased. An increase in feed rate also led to an increase in hardness. In addition, the effects of various greases and coolant oil were studied using the same feed rates; when coolant oil was used, hardness increased, and when grease was applied, hardness decreased.

Keywords:SPIF; single point incremental forming; sheet forming; hardness; ANN; relative importance (RI)

1. Introduction

Incremental Sheet Forming (ISF) is a sheet-forming technique that produces compo- nents through a series of small incremental deformations. ISF is a flexible active manufac- turing process and is economically feasible for low-volume production due to the absence of a punch and die. SPIF is one of the major types of ISF, and it is known as the simplest process variant of incremental sheet-forming technologies. SPIF is an emerging process that has been identified as suitable for use in small-scale production. Trzepieci ´nski et al. [1]

presented a brief overview of state-of-the-art methods of ISF for lightweight materials. The aim of their paper was to guide and inspire researchers by identifying current development trends of valuable contributions in the field of Single Point Incremental Forming (SPIF) of lightweight metallic materials. In SPIF, a rotating tool with a rounded tip at its end is used,

Materials2021,14, 7263. https://doi.org/10.3390/ma14237263 https://www.mdpi.com/journal/materials

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Materials2021,14, 7263 2 of 19

and the desired shape is formed from clamped sheet metal [2]. In the literature [3], a review paper on new advances and future opportunities considered single point incremental to be one of the forming technologies of future-proof materials in aerospace applications.

Furthermore, there is governmental, academic, and business interest in developing new manufacturing technologies, and there is also interest in ISF’s impact on the environment, particularly in what ways and to what extent ISF reduces energy needs [4]. Two exergy analyses of traditional forming and hydroforming of ISF were contrasted by Dittrich et al.

in [5]. After analysing the environmental impact of these forming techniques in the supply chain, they concluded that ISF is significantly less harmful to the environment, particu- larly for prototypes and non-mass production. Sustainability guidelines were developed by Ingarao et al. [6] regarding the advantages and disadvantages of SPIF related to the amount of energy necessary to form sheets and to economic material use in each process.

Ingarao et al. proved that SPIF supports saving material with respect to CO2emissions, because it supports recycling and facilitates novel ways of preparing raw materials. An overview of the history of ISF was written by Emmens et al. [7], Li et al. [8], and Behera et al. [9]: they discussed the enormous benefits and many advantages of SPIF and par- ticularly referenced the flexibility of the process, which allows SPIF to be used in more applications in industries and processes. Hence, SPIF will be considered an essential process for the industry in the future.

By studying the mechanical properties of components formed through SPIF and standardising effective process parameters, the SPIF process can become a significant industrial application embraced by numerous companies. To set optimal input process parameters of SPIF with multiple pure copper sheets, Raju and Sathiya [10] utilised a hybrid optimisation technique by connecting it with Taguchi grey relational analysis and the methodology of the response surface. They showed that the feed rate is the most significant parameter, followed by step depth and tooltip diameter. On the other hand, lubrication plays a vital role in the successful forming of components during the SPIF process. Lubrication reduces friction at the contact zone of the tool and sheet [11]. Recently, Joséet al. [12] studied how mineral oil, sunflower, soybean, and corn lubricants influence friction and wear effects on aluminium parts manufactured using the SPIF process. Using a scanning electron microscope, they found the following: the experimental characterisation of the sample’s surface showed that the worn surface of the metallic material samples produced using vegetable oils increases surface roughness compared to those produced with mineral oils. With respect to aluminium alloy foils, Najm and Paniti [13,14] noted that a flat tool yielded better outcomes than a hemispherical tool in various conditions of the SPIF process. The best geometric accuracy was achieved when the smallest corner radius flat tool was used because a decrease in spring-back was observed. ISF-as-a-Service was introduced by Paniti [15], who distinguished first-order and second-order bottleneck parameters. He described the main capabilities of an incremental sheet-forming service provider in cloud manufacturing. The hardening and normal anisotropy coefficients are the most influential factors on traditional Forming Limit Diagrams (FLDs), as found by Fratini et al. [16] when studying the relationship between material formability and mechanical properties. On the other hand, Zhang [17] concluded that the most influential factor on formability is forming temperature, followed by vertical step depth, sheet thickness, and tooltip diameter.

The above-mentioned results were obtained on Mg alloy sheets formed by using warm incremental sheet forming. Liu et al. [18] asserted that formability and maximum vertical force increase when vertical step-down increases, and they linearly increase when sheet thickness is increased. In their study [19], Li et al. found that mechanical properties and the thinning rate were affected by three parameters of ISF. It was shown that an increase in the tool diameter considerably improved the microhardness of the product’s surface.

An increase in the tool diameter and a decrease in the step size ultimately increase the tensile strength rate. Li et al. claimed that contrary to step size, sheet thickness significantly affects yield strength. In [20], Manco et al. proved that, due to variations in tool path, tool trajectory could be considered an essential parameter for the optimisation of process design

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by comparing the smallest thickness of the sheet with predicted thickness using the sine law. Krasowski et al. [21] analysed and discussed experimental investigations of the effects of selected SPIF parameters on the formability of DC04 sheets and the susceptibility to crack formation on truncated cones produced through SPIF, and they found that lubrication conditions clearly affect the formability of DC04 steel sheets.

At present, many methods of artificial intelligence are used in various applications, in- cluding the metal forming process. More specifically, ANN generates predictive models for end-milling machining, powder metallurgy, and high-speed machining [22–24]. Moreover, machine learning techniques with controlled manufacturing are used to develop various effective predictive models [25–29]. Trzepieci ´nski et al. [30] presented an analysis of the interaction between SPIF process parameters and the main roughness parameters. They found that predictive models of ANNs for Ra and Rz were characterised by performance measures of R2values between 0.657 and 0.979. In other studies, different tool materials and shapes were investigated experimentally to study factors including formability, ge- ometric accuracy [31], and surface roughness [32] on an AlMn1Mg1 sheet formed using SPIF under various forming conditions. The researchers evaluated the performance of an Artificial Neural Network (ANN) and Support Vector Regression (SVR). Two different ANN models were built in the study: an R-squared value with other validation metrics and a feed-forward neural network with a backpropagation algorithm were used. A close cor- respondence was found between predicted roughness, formability, and geometric accuracy in the experimental results. The researchers derived regression equations to analytically predict surface roughness in terms of Ra and Rz. Baruah et al. [33] claimed that lubrication was the largest contributing factor in the process of ISF in all three directions (rolling, transverse, and angular) when surface roughness in ISF is meant to be reduced. In fact, to date, the applied lubricant and the viscosity of the lubricants on the ISF process have not been optimised or discussed, as attested by [5,34,35]. In addition, Kumar and Gulati [34]

claimed that all parameters investigated in their study were significant for forming force except lubricating oil viscosity, and they also noted that surface roughness decreased when viscosity increased [35]. According to the literature, ANN is a helpful tool—before starting new experiments—for predicting and designing predictive models to estimate expected results, behaviour, or direction based on the use of the parameters of the studied process.

Using ANN before starting an actual experiment has the essential benefits of selecting the correct parameters, reducing processing time, increasing efficiency, minimising errors, and comparing actual results with predicted ones so as to reach the best values. In addition, ANN is considered one of the most powerful tools for solving engineering problems by predicting experimental data. In addition, ANN can serve as a valuable means to generate and assess different processes and prepare the final details of tools.

Under normal conditions, the hardness behaviour in SPIF is as follows: formed parts achieve higher hardness than an unformed sheet. Using different path strategies and different forming angles, Al-Attaby et al. [36] showed that the tool path affects the hardness and microstructure of the formed sheet. In all cases relating to the forming angle, hardness increased. Regarding the two-point incremental forming process, Mostafanezhad et al. [37] analysed the formability of aluminium 1050: the scholars used the response surface methodology experimentally. They found that wall angle is the most influential factor with respect to the thinning ratio; initial thickness, followed by step-down, has a significant impact on forming force.

The above-detailed issues, the need for well-defined mechanical properties of SPIF components, and the lack of referent analytical models prompted the authors to investigate the effects of SPIF process variables on the hardness of truncated cones formed from AA1100 aluminium alloy sheets. Moreover, as a novelty and aim contributing to the significance of this paper, different regression equations were derived to determine the hardness of the components of a truncated cone using SPIF. In addition, the Relative Importance (RI) of parameters of SPIF on hardness was assessed and classified by utilising the joint partitioning weight of the built neural network. To the best of the authors’ knowledge

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and according to the literature introduced, such an experimental process has not been reported to date. In this research, the influences of feed rate, various kinds of grease and coolant oil, spindle speed, and tool diameter on the hardness of the AA1100 aluminium alloy sheet formed by SPIF were investigated. Conventionally, AA1100 alloy is employed for radiator components [38]. However, as a final general aim, it was posited that the appropriate selection of properties would improve the application of the AA1100 alloy.

Furthermore, based on the diver’s mechanism of deformation, Song et al. [39] found three different regions of deformation (bending/stretching, shear, and stretch/shear). Based on these research projects, in this study, hardness was measured in three different positions on the inside wall of the cone, and measured data were compared to the primary hardness of the sheet involved in the experiment.

2. Material and Methods 2.1. Workpiece Material

Aluminium and aluminium alloys have become attractive materials for application in the aerospace and automotive industries owing to their beneficial properties. In the experi- ments conducted in this study, single point incremental forming tests were conducted using a blank sheet of AA1100 aluminium alloy were produced by Xuzhou Bozhan Aluminum Technology Co. Ltd, Xuzhou, Jiangsu, China with an initial hardness of 42.87 HV. The initial thickness of the sheet used is 0.6 mm, with an original surface roughness of 0.29µm.

AA1100 aluminium belongs to the 1xxx series with less than 1% alloying elements. The main uses of the 1xxx series aluminium alloys are foil and strip for packaging, chemical equipment, tank car or truck bodies, spun hollowware, and elaborate sheet metal work because of their high corrosion resistance and formability [40]. The 1xxx alloys are essen- tially characterised by superior corrosion resistance, usefulness for fabricating chemical tanks and piping, or their excellent electrical conductivity, as in bus bar applications. These alloys have relatively poor mechanical properties [41].

If strength is not an essential factor, AA1100 aluminium is selected to create fuel tanks, cowlings, and oil tanks of aircraft due to the corrosion resistance and the economic weight.

The before-mentioned grade of aluminium can be utilised to repair aircraft wingtips and tanks because it is weldable [42]. AA1100 commercially pure aluminium is highly resistant to chemical attack and weathering. This low-cost material is characterised by excellent solderability and susceptibility to deep drawing. It is used for high-purity applications such as chemical processing equipment. In addition, examples of common 1xxx series aluminium alloy applications include nameplates, fan blades, flue lining, sheet metal work, spun holloware, and fin stock [43]. It is also used to produce decorative parts, giftware, cooking utensils, rivets, and reflectors. A SPECTROMAXx optical emission spectrometer manufactured by SPECTRO, Kleve, Germany was used to determine the chemical composition of the AA1100 alloy used, and the test of mechanical properties was conducted with a United testing machine according to the ASTM B557M-15 standard test methods for tension check. The results of the tests of the aluminium sheet were compared with the nominal values in the ASM Handbook [44]: these tests show the conformity to the standard composition of the alloy (ISO 19000 standard). The mechanical properties and the chemical composition of the sheet material are shown in Tables1and2, respectively.

Table 1.Mechanical properties of the AA1100 aluminium alloy sheet.

Property Ultimate Tensile

Stress, MPa Yield Strength, MPa Elongation, %

Actual 110 95 20

Nominal 110 103 25

Standard Deviation,σ 0 4 2.5

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Table 2.Chemical composition of the AA1100 aluminium alloy sheet (in wt.%).

Element Si Fe Cu Mn Mg Cr Ni Zn Ti Pb B Sn V Al

Actual 0.110 0.482 0.004 0.005 0.001 0.0005 0.004 0.021 0.021 0.0005 0.003 0.001 0.014 balance

Nominal 0.5 0.5 0.2 0.04 0.01 Other 0.15 max balance

2.2. Experimental Setup

In this study, a Boxford 300VMCi milling machine built by Boxford in Halifax, UK with 0.01 mm accuracy was used. The ISO format using G and M codes was used to program a cone shape with large and small diameters of 80 and 10 mm, respectively. An inward spiral path strategy was used to deform the cone part, in which case a spiral tool trajectory is advantageous to the successful forming of the same parts [45]. The strategy utilised in this study was developed by Skjoedt et al. [46] to overcome the difficulty of reaching maximum axial loads at each layer (step down) and to prevent the appearance of a line on the inner side of the formed part. A wall angle of 45, a context contour of 0.5 mm for the step size, and an inward spiral path were applied, as shown in Figure1.

Table 1. Mechanical properties of the AA1100 aluminium alloy sheet.

Property Ultimate Tensile

Stress, MPa Yield Strength, MPa Elongation, %

Actual 110 95 20

Nominal 110 103 25

Standard Deviation, σ 0 4 2.5

Table 2. Chemical composition of the AA1100 aluminium alloy sheet (in wt.%).

Element Si Fe Cu Mn Mg Cr Ni Zn Ti Pb B Sn V Al

Actual 0.110 0.482 0.004 0.005 0.001 0.0005 0.004 0.021 0.021 0.0005 0.003 0.001 0.014 balance

Nominal 0.5 0.5 0.2 0.04 0.01 Other 0.15 max balance

2.2. Experimental Setup

In this study, a Boxford 300VMCi milling machine built by Boxford in Halifax, UK with 0.01 mm accuracy was used. The ISO format using G and M codes was used to pro- gram a cone shape with large and small diameters of 80 and 10 mm, respectively. An inward spiral path strategy was used to deform the cone part, in which case a spiral tool trajectory is advantageous to the successful forming of the same parts [45]. The strategy utilised in this study was developed by Skjoedt et al. [46] to overcome the difficulty of reaching maximum axial loads at each layer (step down) and to prevent the appearance of a line on the inner side of the formed part. A wall angle of 45°, a context contour of 0.5 mm for the step size, and an inward spiral path were applied, as shown in Figure 1.

(a) (b)

Figure 1. (a) CAD geometry and dimensions of the experimental product and (b) view of an inward spiral path.

In the SPIF process, only one tool can be used, and the feed rate, spindle speed, lub- ricant, and forming conditions should be selected beforehand. Furthermore, in the current study, the mentioned parameters were considered parametric values and were changed in the subsequent part forming. A primary step was conducted to select the best values of these parameters to fix them in the subsequent forming process, and only one of these parameters was changed in each forming group. To this end, a matrix of 3 factors with the same levels (feed rate, spindle speed, and tool diameter) was applied in the first step. The best values of feed rate, spindle speed, and tool diameter were chosen depending on the best geometrical accuracy and maximum depth. In the second step, the best values se- lected from the first step were applied in order to study the coolant type.

Forming tools with different diameters (4, 6, 8, and 10 mm) were used in the experi- ment, as shown in Figure 2a. The tools used in the experiment are made of carbon steel

Figure 1.(a) CAD geometry and dimensions of the experimental product and (b) view of an inward spiral path.

In the SPIF process, only one tool can be used, and the feed rate, spindle speed, lubricant, and forming conditions should be selected beforehand. Furthermore, in the current study, the mentioned parameters were considered parametric values and were changed in the subsequent part forming. A primary step was conducted to select the best values of these parameters to fix them in the subsequent forming process, and only one of these parameters was changed in each forming group. To this end, a matrix of 3 factors with the same levels (feed rate, spindle speed, and tool diameter) was applied in the first step. The best values of feed rate, spindle speed, and tool diameter were chosen depending on the best geometrical accuracy and maximum depth. In the second step, the best values selected from the first step were applied in order to study the coolant type.

Forming tools with different diameters (4, 6, 8, and 10 mm) were used in the experi- ment, as shown in Figure2a. The tools used in the experiment are made of carbon steel with a hardness of 30 HRC and are 100 mm in total length. Plain carbon steel was used for manufacturing the clamping rig, which was fixed to the CNC machine table with a simple-to-use fixture system, as shown in Figure2b.

A digital Vickers microhardness tester supplied by TIME Group Inc., Beijing, China was used to measure the hardness of the component formed using SPIF (see Figure3a) based on Equation (1). For each set, three products were experimentally formed to study the process parameters of different forming conditions (see Figure3b). The hardness of

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each part was measured at three zones: the upper, middle, and lower zones along the inner wall of the formed part. Figure3c shows a formed part after it was cut to the desired shape in the proper size for the preparation of the test samples and for establishing the three zones of the hardness measurement. The hardness measurement was repeated three times at different points inside each mentioned zone. The hardness value of each zone was calculated as the average value of the selected zone hardness. The average hardness value of the three zones was considered the average value of the measured component. The appropriate piece of the section was mounted by a mounting press device and polished by a Metaserv type 250/RP device manufactured in (Buehler, Lake Bluff, IL, USA) before hardness was measured (see Figure3d).

Hv=1854.4 F

d2 (1)

whereFis penetration force (N), anddis average diagonal distance (d1 + d2)/2.

Materials 2021, 14, x 6 of 20

with a hardness of 30 HRC and are 100 mm in total length. Plain carbon steel was used for manufacturing the clamping rig, which was fixed to the CNC machine table with a simple- to-use fixture system, as shown in Figure 2b.

(a) (b)

Figure 2. (a) Forming tools with different diameters, (b) fixture rig on the CNC machine table.

A digital Vickers microhardness tester supplied by TIME Group Inc., Beijing, China was used to measure the hardness of the component formed using SPIF (see Figure 3a) based on Equation (1). For each set, three products were experimentally formed to study the process parameters of different forming conditions (see Figure 3b). The hardness of each part was measured at three zones: the upper, middle, and lower zones along the inner wall of the formed part. Figure 3c shows a formed part after it was cut to the desired shape in the proper size for the preparation of the test samples and for establishing the three zones of the hardness measurement. The hardness measurement was repeated three times at different points inside each mentioned zone. The hardness value of each zone was calculated as the average value of the selected zone hardness. The average hardness value of the three zones was considered the average value of the measured component.

The appropriate piece of the section was mounted by a mounting press device and pol- ished by a Metaserv type 250/RP device manufactured in (Buehler, Lake Bluff, IL, USA) before hardness was measured (see Figure 3d).

𝐻

𝑣

= 1854.4 𝐹

𝑑

2 (1)

where F is penetration force (N), and d is average diagonal distance (d1 + d2)/2.

Figure 2.(a) Forming tools with different diameters, (b) fixture rig on the CNC machine table.

Materials 2021, 14, x 7 of 20

Figure 3. (a) Digital microhardness device, (b) formed parts, (c) three zones of hardness measure- ment, (d) hardness test sample of the formed part.

For hardness measurement, the hardness tester was calibrated before testing using the calibration standard block, and 100 N was applied on the formed part with a Vickers diamond pyramid indenter for 15 s. The results were recorded automatically on a digital screen after the adjustment of the rhomb corner had been triggered by the indenter.

There is no internationally accepted term for the definition of Environmentally Ac- ceptable Lubricants (EALs), and they still lack standardisation. The American Society for Testing and Materials (ASTM) used “environmentally acceptable” as a phrase for defining EALs [47]. There is an overall trend towards using EALs. In the present study, different coolant types (four different grease types, as shown in Figure 4a–d, and one coolant oil) were used to carry out the experiment. Supergrees EP2 and Kaucuklu grease produced by Petrol Ofisi, Istanbul, Turkey, Zinol grease from Universal Lubricants (ZINOL) L.L.C, Sharjah, United Arab Emirates, Gp Grease Calcium type was produced by United Grease

& Lubricants Co. LLC based in Ajman, United Arab Emirates, and the coolant oil was also by Petrol Ofisi, Istanbul, Turkey. Table 3 lists grease properties based on their commercial name and standard denominations, and Table 4 presents coolant oil properties. It is worth mentioning that viscosity values of different greases were assumed based on the ISO 3448:1992 standard for viscosity grading systems [48].

Figure 4. Different types of grease: (a) EP2, (b) Kaucuklu, (c) Zinol, (d) Gp Grease Calcium.

Figure 3.(a) Digital microhardness device, (b) formed parts, (c) three zones of hardness measurement, (d) hardness test sample of the formed part.

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For hardness measurement, the hardness tester was calibrated before testing using the calibration standard block, and 100 N was applied on the formed part with a Vickers diamond pyramid indenter for 15 s. The results were recorded automatically on a digital screen after the adjustment of the rhomb corner had been triggered by the indenter.

There is no internationally accepted term for the definition of Environmentally Ac- ceptable Lubricants (EALs), and they still lack standardisation. The American Society for Testing and Materials (ASTM) used “environmentally acceptable” as a phrase for defining EALs [47]. There is an overall trend towards using EALs. In the present study, different coolant types (four different grease types, as shown in Figure4a–d, and one coolant oil) were used to carry out the experiment. Supergrees EP2 and Kaucuklu grease produced by Petrol Ofisi, Istanbul, Turkey, Zinol grease from Universal Lubricants (ZINOL) L.L.C, Sharjah, United Arab Emirates, Gp Grease Calcium type was produced by United Grease

& Lubricants Co. LLC based in Ajman, United Arab Emirates, and the coolant oil was also by Petrol Ofisi, Istanbul, Turkey. Table3lists grease properties based on their commer- cial name and standard denominations, and Table4presents coolant oil properties. It is worth mentioning that viscosity values of different greases were assumed based on the ISO 3448:1992 standard for viscosity grading systems [48].

Figure 3. (a) Digital microhardness device, (b) formed parts, (c) three zones of hardness measure- ment, (d) hardness test sample of the formed part.

For hardness measurement, the hardness tester was calibrated before testing using the calibration standard block, and 100 N was applied on the formed part with a Vickers diamond pyramid indenter for 15 s. The results were recorded automatically on a digital screen after the adjustment of the rhomb corner had been triggered by the indenter.

There is no internationally accepted term for the definition of Environmentally Ac- ceptable Lubricants (EALs), and they still lack standardisation. The American Society for Testing and Materials (ASTM) used “environmentally acceptable” as a phrase for defining EALs [47]. There is an overall trend towards using EALs. In the present study, different coolant types (four different grease types, as shown in Figure 4a–d, and one coolant oil) were used to carry out the experiment. Supergrees EP2 and Kaucuklu grease produced by Petrol Ofisi, Istanbul, Turkey, Zinol grease from Universal Lubricants (ZINOL) L.L.C, Sharjah, United Arab Emirates, Gp Grease Calcium type was produced by United Grease

& Lubricants Co. LLC based in Ajman, United Arab Emirates, and the coolant oil was also by Petrol Ofisi, Istanbul, Turkey. Table 3 lists grease properties based on their commercial name and standard denominations, and Table 4 presents coolant oil properties. It is worth mentioning that viscosity values of different greases were assumed based on the ISO 3448:1992 standard for viscosity grading systems [48].

Figure 4. Different types of grease: (a) EP2, (b) Kaucuklu, (c) Zinol, (d) Gp Grease Calcium. Figure 4.Different types of grease: (a) EP2, (b) Kaucuklu, (c) Zinol, (d) Gp Grease Calcium.

Table 3.Selected properties of the greases used.

Grease Type ISO Viscosity Grade Average Dropping Point,C

(at 25C) Flash Point,C Viscosity at 40C, mm2/s

EP2 ISO VG 15 90 180 15

Kaucuklu ISO VG 22 88 172 22

Zinol ISO VG 32 88 170 32

Gp Grease Calcium ISO VG 46 58 60 46

Table 4.Selected properties of the coolant oil used.

Acidity, pH Kinematic Viscosity at 29C, mm2/s Boiling Point,C

1.086 1.086 95

Lubricants cannot be used in forming processes where high loads are applied, and thus, Syahrullail et al. [49] suggested using an appropriate additive to solve this problem.

Consequently, the difference between using coolant oil and grease is that grease forms a mixture with small disintegrating particles (debris) of either the formed sheet or, in rare cases, the tool. Due to heat generation, sometimes the debris repeatedly sticks to the sheet surface or passes between the tool and the formed sheet. Diabb et al. [50] observed aluminium flakes in the used lubricant: this phenomenon was caused by wear adhesion on alloy sheets of SPIF components. In the case of coolant oil, which flows continuously on the sheet, debris can be washed away from the forming zone. However, when grease is used, a smoother surface can be produced compared to the scenario where coolant oil is used due to the flattening and roughening effects exerted by the debris, as stated in [51].

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On the other hand, coolant oil continuously flows during the forming process, whereas grease is applied on the sheet surface only once at the beginning of the process. In other words, coolant oil has higher exergy than grease due to the difference in the amount of material used, which means that an increased environmental impact is observable.

Figure5a,b illustrate the processes of using grease and coolant oil.

Materials 2021, 14, x 8 of 20

Table 3. Selected properties of the greases used.

Grease Type ISO Viscosity Grade

Average Dropping Point, °C (at 25 °C)

Flash Point, °C Viscosity at 40 °C, mm

2

/s

EP2 ISO VG 15 90 180 15

Kaucuklu ISO VG 22 88 172 22

Zinol ISO VG 32 88 170 32

Gp Grease Calcium ISO VG 46 58 60 46

Table 4. Selected properties of the coolant oil used.

Acidity, pH Kinematic Viscosity at 29 °C, mm

2

/s Boiling Point, °C

1.086 1.086 95

Lubricants cannot be used in forming processes where high loads are applied, and thus, Syahrullail et al. [49] suggested using an appropriate additive to solve this problem.

Consequently, the difference between using coolant oil and grease is that grease forms a mixture with small disintegrating particles (debris) of either the formed sheet or, in rare cases, the tool. Due to heat generation, sometimes the debris repeatedly sticks to the sheet surface or passes between the tool and the formed sheet. Diabb et al. [50] observed alu- minium flakes in the used lubricant: this phenomenon was caused by wear adhesion on alloy sheets of SPIF components. In the case of coolant oil, which flows continuously on the sheet, debris can be washed away from the forming zone. However, when grease is used, a smoother surface can be produced compared to the scenario where coolant oil is used due to the flattening and roughening effects exerted by the debris, as stated in [51].

On the other hand, coolant oil continuously flows during the forming process, whereas grease is applied on the sheet surface only once at the beginning of the process.

In other words, coolant oil has higher exergy than grease due to the difference in the amount of material used, which means that an increased environmental impact is observ- able. Figure 5a,b illustrate the processes of using grease and coolant oil.

(a) (b)

Figure 5. (a) Forming process using grease, (b) forming process using coolant oil.

Four different tool rotation speeds (500, 1000, 1500, and 2000 rpm) were used to study hardness behaviour. In addition, in the scope of the current experiments, four different feed rates (200, 400, 600, and 800 mm/min) were implemented to investigate the effects of changes in the feed rate on sheet hardness.

3. Results and Discussion 3.1. Feed Rate

Four different feed rates were used with different lubricants (oil and grease). At the same time, other experimental parameters were fixed: the tool speed was 2000 rpm, the

Figure 5.(a) Forming process using grease, (b) forming process using coolant oil.

Four different tool rotation speeds (500, 1000, 1500, and 2000 rpm) were used to study hardness behaviour. In addition, in the scope of the current experiments, four different feed rates (200, 400, 600, and 800 mm/min) were implemented to investigate the effects of changes in the feed rate on sheet hardness.

3. Results and Discussion 3.1. Feed Rate

Four different feed rates were used with different lubricants (oil and grease). At the same time, other experimental parameters were fixed: the tool speed was 2000 rpm, the tool diameter was 10 mm, and coolant oil was used. Table5and Figure6a,b show the results of hardness measurements for different feed rates. Changing the lubricant type resulted in inverse values of hardness: it increased when the feed rate was increased and coolant oil was used, and it decreased when grease was used.

An increase in feed rate led to an increase in hardness, and this was inversely pro- portional to formability. The increase in feed rate caused a decrease in formability, as mentioned in [52]. A decrease in hardness is due to changes in surface asperities because the peaks of the aspirates formed by the generated debris shoot and break. By attach- ing the debris to the tool and cultivating the sheet surface, new grooves can be created, and the sharp peaks of the asperities can likewise be crashed. Finally, through contin- uous cultivation and crashing, the contact area between the tool and the formed sheet will increase.

Table 5.Effects of different feed rates on hardness.

Feed Rate, mm/min

Hardness HV

Coolant Oil Grease

Top Middle Bottom Standard

Deviation,σ Top Middle Bottom Standard

Deviation,σ

200 43.89 40.40 39.02 2.0494 63.30 58.61 50.56 5.2610

400 39.16 43.61 41.78 1.8262 59.80 56.70 49.13 4.4816

600 44.08 46.44 48.22 1.6957 51.29 53.17 44.70 3.6317

800 47.76 53.84 49.54 2.5522 43.99 45.72 45.50 0.7689

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tool diameter was 10 mm, and coolant oil was used. Table 5 and Figure 6a,b show the results of hardness measurements for different feed rates. Changing the lubricant type resulted in inverse values of hardness: it increased when the feed rate was increased and coolant oil was used, and it decreased when grease was used.

Table 5. Effects of different feed rates on hardness.

Feed Rate, mm/min

Hardness HV

Coolant Oil Grease

Top Middle Bottom Standard

Deviation, σ Top Middle Bottom Standard Deviation, σ

200 43.89 40.40 39.02 2.0494 63.30 58.61 50.56 5.2610 400 39.16 43.61 41.78 1.8262 59.80 56.70 49.13 4.4816 600 44.08 46.44 48.22 1.6957 51.29 53.17 44.70 3.6317 800 47.76 53.84 49.54 2.5522 43.99 45.72 45.50 0.7689

Figure 6. (a) Effects of different feed rates on hardness of formed sheet when using coolant oil, (b) effects of varied feed rates on hardness of formed sheet when using grease.

200 400 600 800

38 40 42 44 46 48 50 52 54

Hardness (HV)

Feed rate (mm/min)

Average of Top Point Hardness Average of Middle Point Hardness Average of Bottom Point Hardness Average of Sheet Hardness

a

200 400 600 800

42 44 46 48 50 52 54 56 58 60 62 64

Hardness (HV)

Feed rate (mm/min)

Average of Top Point Hardness Average of Middle Point Hardness Average of Bottom Point Hardness Average of Sheet Hardness

b

Figure 6.(a) Effects of different feed rates on hardness of formed sheet when using coolant oil, (b) effects of varied feed rates on hardness of formed sheet when using grease.

Hol et al. [53] mentioned that, in the case of normal forces, the sheet surface asperities are in the plastic condition, and they are further affected by only a little stress in the underlying bulk material. They claim that this stress is perpendicular to the normal force and generates increased plastic deformation of asperities. Finally, because of the enormous strain of the underlying material, this situation leads to an increased contact area, which is recognised as a decrease in effective hardness.

3.2. Tool Speed

Table6lists different tool rotation speeds with the experimentally obtained hardness values. Figure7shows that an increase in tool speed led to an increase in hardness. High speed causes the resulting particles to impact the surface of the sheet faster than in the case of low speeds, and this results in the hardening of the surface. On the other hand, in the case of high tool speeds, the tool head, in the same contact area, travels on the sheet with

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Materials2021,14, 7263 10 of 19

more passes than a tool at low speeds. Due to stretching with longitudinal deformation, the sheet material seems to be undergoing cold working conditions. Cold working creates a different type of crystal deformation, such as compressing, twisting, and bending, and this results in comparatively uniform plain crystalline particles. New imperfections created by these movements result in more resistance and, finally, increase hardness.

Table 6.Effect of different speed values on hardness.

Tool Speed, rpm

Hardness HV

Top Middle Bottom Standard

Deviation,σ

500 45.83 41.78 40.10 2.4050

1000 50.50 47.48 42.75 3.1895

1500 56.83 55.96 45.90 4.9601

2000 61.58 75.51 57.71 7.6439

Materials 2021, 14, x 10 of 20

An increase in feed rate led to an increase in hardness, and this was inversely pro- portional to formability. The increase in feed rate caused a decrease in formability, as men- tioned in [52]. A decrease in hardness is due to changes in surface asperities because the peaks of the aspirates formed by the generated debris shoot and break. By attaching the debris to the tool and cultivating the sheet surface, new grooves can be created, and the sharp peaks of the asperities can likewise be crashed. Finally, through continuous cultiva- tion and crashing, the contact area between the tool and the formed sheet will increase.

Hol et al. [53] mentioned that, in the case of normal forces, the sheet surface asperities are in the plastic condition, and they are further affected by only a little stress in the un- derlying bulk material. They claim that this stress is perpendicular to the normal force and generates increased plastic deformation of asperities. Finally, because of the enor- mous strain of the underlying material, this situation leads to an increased contact area, which is recognised as a decrease in effective hardness.

3.2. Tool Speed

Table 6 lists different tool rotation speeds with the experimentally obtained hardness values. Figure 7 shows that an increase in tool speed led to an increase in hardness. High speed causes the resulting particles to impact the surface of the sheet faster than in the case of low speeds, and this results in the hardening of the surface. On the other hand, in the case of high tool speeds, the tool head, in the same contact area, travels on the sheet with more passes than a tool at low speeds. Due to stretching with longitudinal defor- mation, the sheet material seems to be undergoing cold working conditions. Cold working creates a different type of crystal deformation, such as compressing, twisting, and bend- ing, and this results in comparatively uniform plain crystalline particles. New imperfec- tions created by these movements result in more resistance and, finally, increase hardness.

Table 6. Effect of different speed values on hardness.

Tool Speed, rpm Hardness HV

Top Middle Bottom Standard Deviation, σ

500 45.83 41.78 40.10 2.4050

1000 50.50 47.48 42.75 3.1895

1500 56.83 55.96 45.90 4.9601

2000 61.58 75.51 57.71 7.6439

Figure 7. Effect of different tool speeds on hardness of formed sheet (feed rate: 600 mm/min; tool diameter: 10 mm; coolant: oil).

500 1000 1500 2000

40 45 50 55 60 65 70 75 80

Hardness (HV)

Tool Speed (rpm)

Average of Top Point Hardness Average of Middle Point Hardness Average of Bottom Point Hardness Average of Sheet Hardness

Figure 7.Effect of different tool speeds on hardness of formed sheet (feed rate: 600 mm/min; tool diameter: 10 mm; coolant: oil).

3.3. Tool Diameter

The effects of tool diameter on hardness are presented in Table7and in Figure8.

Decreases in values are due to increases in tool diameter. McAnulty et al. [54] found differ- ent behaviours for the effects of changes in tool diameter on formability. Asgari et al. [55]

concluded that a tool diameter of 3 mm results in increased hardness in an aluminium alloy 1100-O sheet relative to 5 or 10 mm tool diameters. A decrease in tool diameter from 10 to 3 mm causes ultimate tensile stress and yield stress to decrease by 7% and 24%, respec- tively. Furthermore, a reduction in the tool diameter causes a decrease in grain size [55].

Shrivastava and Tandon [56] discussed various parameters of the pre-production sheet and studied the effects of such parameters on the ISF process and on the final properties of products. They claimed that the forces needed to form the sheet in ISF are affected by grain size. Increasing the grain size leads to a decrease in forming forces, yield stress, and hardness [56]. The researchers used different tools for forming, and all of the formed parts showed decreased hardness irrespective of the diameter of the applied tools. The results of this study show that hardness decreased in the case of any diameter of the tool irrespective of the hardness value at each point. A tool diameter of 4 mm showed higher hardness than

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Materials2021,14, 7263 11 of 19

other diameters at all points. Tool diameters of 10 and 8 mm, on the other hand, produced lower hardness values than tool diameters of 6 and 4 mm. In addition, larger tools, which passed through the formed sheet more times than smaller tools, made the material of the formed part softer (and also caused more heating through increased friction).

Table 7.Effects of different tool diameters on hardness.

Tool Diameter, mm

Hardness HV

Top Middle Bottom Standard

Deviation,σ

4 75.51 57.71 66.61 7.2668

6 56.33 50.65 53.01 2.3299

8 43.22 40.62 44.26 1.5308

10 41.78 40.10 42.57 1.0300

3.3. Tool Diameter

The effects of tool diameter on hardness are presented in Table 7 and in Figure 8.

Decreases in values are due to increases in tool diameter. McAnulty et al. [54] found dif- ferent behaviours for the effects of changes in tool diameter on formability. Asgari et al.

[55] concluded that a tool diameter of 3 mm results in increased hardness in an aluminium alloy 1100-O sheet relative to 5 or 10 mm tool diameters. A decrease in tool diameter from 10 to 3 mm causes ultimate tensile stress and yield stress to decrease by 7% and 24%, respectively. Furthermore, a reduction in the tool diameter causes a decrease in grain size [55]. Shrivastava and Tandon [56] discussed various parameters of the pre-production sheet and studied the effects of such parameters on the ISF process and on the final prop- erties of products. They claimed that the forces needed to form the sheet in ISF are affected by grain size. Increasing the grain size leads to a decrease in forming forces, yield stress, and hardness [56]. The researchers used different tools for forming, and all of the formed parts showed decreased hardness irrespective of the diameter of the applied tools. The results of this study show that hardness decreased in the case of any diameter of the tool irrespective of the hardness value at each point. A tool diameter of 4 mm showed higher hardness than other diameters at all points. Tool diameters of 10 and 8 mm, on the other hand, produced lower hardness values than tool diameters of 6 and 4 mm. In addition, larger tools, which passed through the formed sheet more times than smaller tools, made the material of the formed part softer (and also caused more heating through increased friction).

Table 7. Effects of different tool diameters on hardness.

Tool Diameter, mm Hardness HV

Top Middle Bottom Standard Deviation, σ

4 75.51 57.71 66.61 7.2668

6 56.33 50.65 53.01 2.3299

8 43.22 40.62 44.26 1.5308

10 41.78 40.10 42.57 1.0300

Figure 8. Effect of different tool diameters on hardness of formed sheet (feed rate: 600 mm/min; tool speed: 2000 rpm; coolant: oil).

4 6 8 10

40 45 50 55 60 65 70 75 80

Hardness (HV)

Tool Diameter (mm)

Average of Top Point Hardness Average of Middle Point Hardness Average of Bottom Point Hardness Average of Sheet Hardness

Figure 8. Effect of different tool diameters on hardness of formed sheet (feed rate: 600 mm/min; tool speed: 2000 rpm;

coolant: oil).

3.4. Grease Grade

Table8and Figure9show the impact of different greases on the hardness results. The grease with the highest drop point resulted in the lowest hardness and vice versa. The grease type named “Gp Grease Calcium-ISO VG 46” provided the highest hardness (with the lowest drop point): this was due to the fact that this grease entered between the tool and the formed sheet and cooled the local forming zone faster. Regarding the properties of different greases, it is shown that the use of the grease with a higher flash point resulted in a more stable hardness value. In fact, it can be noted that the use of grease rather than the use of coolant oil produced more homogeneous hardness values at different points of the same sheet, with a slight difference in this conclusion for coolant oil compared to Gp Grease Calcium type grease.

3.5. Regression Equations to Calculate the Hardness of SPIF Components

Regression enables one to find an alternative method to quickly and more economi- cally calculate SPIF components’ hardness, rather than having to resort to an experimental process. In view of this, in our experiments, regression equations capable of calculating

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Materials2021,14, 7263 12 of 19

the hardness of SPIF were used instead of actual measurements. Consequently, differ- ent equations were used in this study: Equation (2) Linear Cross-Validation Regression, (3) Linear Cross-Validation with Multiple Regression of Viscosity, (4) Multiple Regression, and (5) Equation Based on Biases and Weight. These equations are as follows:

Table 8.Effects of different grease types on hardness.

Grease Type ISO

Viscosity Grade

Average Dropping Point

(at 25C) Flash Point,C

Hardness HV

Top Middle Bottom Standard Deviation,σ

Gp Grease Calcium ISO VG 15 58 60 46.81 72.00 56.95 10.3487

Zinol ISO VG 22 88 170 46.34 42.70 40.74 2.3202

Kaucuklu ISO VG 32 88 172 42.73 38.12 40.62 1.8843

EP2 ISO VG 46 90 180 45.81 43.30 38.18 3.1751

Materials 2021, 14, x 12 of 20

3.4. Grease Grade

Table 8 and Figure 9 show the impact of different greases on the hardness results.

The grease with the highest drop point resulted in the lowest hardness and vice versa. The grease type named “Gp Grease Calcium-ISO VG 46” provided the highest hardness (with the lowest drop point): this was due to the fact that this grease entered between the tool and the formed sheet and cooled the local forming zone faster. Regarding the properties of different greases, it is shown that the use of the grease with a higher flash point resulted in a more stable hardness value. In fact, it can be noted that the use of grease rather than the use of coolant oil produced more homogeneous hardness values at different points of the same sheet, with a slight difference in this conclusion for coolant oil compared to Gp Grease Calcium type grease.

Table 8. Effects of different grease types on hardness.

Grease Type

ISO Viscosity

Grade

Average Dropping

Point (at 25 °C)

Flash Point, °C

Hardness HV Top Middle Bottom

Standard Deviation,

σ Gp Grease Calcium ISO VG 15 58 60 46.81 72.00 56.95 10.3487

Zinol ISO VG 22 88 170 46.34 42.70 40.74 2.3202 Kaucuklu ISO VG 32 88 172 42.73 38.12 40.62 1.8843 EP2 ISO VG 46 90 180 45.81 43.30 38.18 3.1751

Figure 9. Effects of different grease types on hardness of formed sheet (feed rate: 600 mm/min; tool speed: 2000 rpm; tool diameter: 10 mm).

3.5. Regression Equations to Calculate the Hardness of SPIF Components

Regression enables one to find an alternative method to quickly and more economi- cally calculate SPIF components’ hardness, rather than having to resort to an experimental process. In view of this, in our experiments, regression equations capable of calculating the hardness of SPIF were used instead of actual measurements. Consequently, different equations were used in this study: Equation (2) Linear Cross-Validation Regression, (3) Linear Cross-Validation with Multiple Regression of Viscosity, (4) Multiple Regression, and (5) Equation Based on Biases and Weight. These equations are as follows:

Linear Cross-Validation Regression:

58 88 88 90

60 170 172 180

36 40 44 48 52 56 60 64 68 72

Flash point (°C)

Hardness (HV)

Average drop point (at 25 °C)

Average of Top Point Hardness Average of Middle Point Hardness Average of Bottom Point Hardness Average of Sheet Hardness

Figure 9.Effects of different grease types on hardness of formed sheet (feed rate: 600 mm/min; tool speed: 2000 rpm; tool diameter: 10 mm).

Linear Cross-Validation Regression:

H=FrCoe f f×Fr+SCoe f f×S+DCoe f f ×D+LCoe f f ×Lv+C /4

H= (0.0658×Fr+0.0028×S−9.3993×D+0.2829×Lv+234.7775)/4 (2) Linear Cross-Validation with Multiple Regression of Viscosity:

H=FrCoe f f×Fr+SCoe f f×S+DCoe f f×D+ (LCoe f f1×LvLCoe f f2×Lv2 +C)/4 H= 0.0749×Fr+0.007482×S8.2277×D+ 3.5691×Lv0.0950×Lv2

+217.7624

/4 (3) Multiple Regression:

H=FrCoe f f1 ×Fr−FrCoe f f2×Fr2) + (SCoe f f1×S−SCoe f f2×S2) + (DCoe f f1×D2−DCoe f f2×D) + (LCoe f f1×Lv2

−LCoe f f2×Lv) +C

H= (0.029255×Fr−0.000010×Fr2) + (0.0278×S−0.000009×S2)

−(17.4122×D−1.0414×D2)

−(0.9343×Lv−0.0244×Lv2) +87.4763

(4)

Equation Based on Biases and Weights:

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Materials2021,14, 7263 13 of 19

𝐻 = (𝐹𝑟𝐶𝑜𝑒𝑓𝑓 × 𝐹𝑟 + 𝑆𝐶𝑜𝑒𝑓𝑓× 𝑆 + 𝐷𝐶𝑜𝑒𝑓𝑓× 𝐷 + 𝐿𝐶𝑜𝑒𝑓𝑓× 𝐿𝑣+ 𝐶)/4

(2) 𝐻 = (0.0658 × 𝐹𝑟 + 0.0028 × 𝑆 − 9.3993 × 𝐷 + 0.2829 × 𝐿𝑣+ 234.7775)/4 Linear Cross-Validation with Multiple Regression of Viscosity:

𝐻 = (𝐹𝑟𝐶𝑜𝑒𝑓𝑓 × 𝐹𝑟 + 𝑆𝐶𝑜𝑒𝑓𝑓× 𝑆 + 𝐷𝐶𝑜𝑒𝑓𝑓× 𝐷 + (𝐿𝐶𝑜𝑒𝑓𝑓1× 𝐿𝑣− 𝐿𝐶𝑜𝑒𝑓𝑓2× 𝐿𝑣2) + 𝐶)/4 (3)

𝐻 = (0.0749 × 𝐹𝑟 + 0.007482 × 𝑆 − 8.2277 × 𝐷 + (3.5691 × 𝐿𝑣− 0.0950 × 𝐿𝑣2

) + 217.7624)/4

Multiple Regression:

𝐻 = (𝐹𝑟𝐶𝑜𝑒𝑓𝑓1× 𝐹𝑟 − 𝐹𝑟𝐶𝑜𝑒𝑓𝑓2× 𝐹𝑟2) + (𝑆𝐶𝑜𝑒𝑓𝑓1× 𝑆 − 𝑆𝐶𝑜𝑒𝑓𝑓2× 𝑆2) + (𝐷𝐶𝑜𝑒𝑓𝑓1× 𝐷2− 𝐷𝐶𝑜𝑒𝑓𝑓2× 𝐷) + (𝐿𝐶𝑜𝑒𝑓𝑓1× 𝐿𝑣2

− 𝐿𝐶𝑜𝑒𝑓𝑓2× 𝐿𝑣) + 𝐶

(4) 𝐻 = (0.029255 × 𝐹𝑟 − 0.000010 × 𝐹𝑟2) + (0.0278 × 𝑆 − 0.000009 × 𝑆2)

− (17.4122 × 𝐷 − 1.0414 × 𝐷2)

− (0.9343 × 𝐿𝑣− 0.0244 × 𝐿𝑣2) + 87.4763

Equation Based on Biases and Weights:

𝐻 = 𝑏2 + 𝐿𝑊 × 𝐸𝑥𝑝(−(𝑏1+𝐼𝑊 ×𝑥)2)

(5)

𝐻= 3.9206 + [𝐿𝑊] × 𝑒𝑥𝑝(

-

([ -5.1413 1.2616 0.6642 2.7010 1.5268 -2.5527 0.9677 0.9160 2.3191 -4.4413]

+ [

-1.1773 -0.7032 -1.7944 -1.8489 1.2188 2.0108 -0.6296 1.9369 0.7717 0.3779

-1.7346 -1.1106 0.1240 0.7292 0.0289 -0.3600 0.6209 -2.3675 -0.6774 -1.6394

0.3222 -0.2106 -0.1155 1.1132 2.3911 -0.5010 -1.7080 0.0188 0.4250 -0.6822 0.1749 -0.6833 -0.8397 1.7357 -1.2086 -0.6854 -0.8242 1.5373 -1.4357 0.2100

] × [

x 𝐹𝑟

𝑆 𝐷 𝐿]

) 2

)

where LW = [6.4552 -2.1276 2.7984 7.8625 4.7908 4.3514 -6.4366 -4.2600 2.3087 4.7381], H is hardness, Fr is feed rate, S is spindle speed, D is tool diameter, LV is viscosity of the lubri- cant, C is the intercept, and Coeff is a coefficient.

Many different validation metrics are used for assessing and measuring the agree- ment between a predictive model and physical observations with the aim of selecting the best models or equations, and choosing the proper validation metric can be a crucial point and a challenge for evaluating results. In this study, the equations developed were com- pared and validated with the validation metrics listed in Table 9. In order to check the equations in question, different validation metrics were used to test performance on the basis of the results of the equations used in the hardness calculation. The criteria of vali- dation consist in minimising error. To this end, Root Mean Square Error (RMSE) and Mean Absolute Error (MAE) were used for validation in this study. RMSE can be more sensitive to the error in case the MAE is more stable. However, RMSE and MAE are more accurate evaluation metrics compared to other metrics [57]. The equation’s more reliable perfor- mance is guaranteed by a condition where MAE and RMSE values are close to 0. Never- theless, the large variance between RMSE and MAE values represents significant varia- tions in error distribution. Consequently, Mean Relative Error (MRE) was used to measure the precision of the equations applied.

(5) whereLW= [6.4552−2.1276 2.7984 7.8625 4.7908 4.3514−6.4366−4.2600 2.3087 4.7381], His hardness,Fris feed rate,Sis spindle speed,Dis tool diameter,LVis viscosity of the lubricant,Cis the intercept, andCoeff is a coefficient.

Many different validation metrics are used for assessing and measuring the agreement between a predictive model and physical observations with the aim of selecting the best models or equations, and choosing the proper validation metric can be a crucial point and a challenge for evaluating results. In this study, the equations developed were compared and validated with the validation metrics listed in Table9. In order to check the equations in question, different validation metrics were used to test performance on the basis of the results of the equations used in the hardness calculation. The criteria of validation consist in minimising error. To this end, Root Mean Square Error (RMSE) and Mean Absolute Error (MAE) were used for validation in this study. RMSE can be more sensitive to the error in case the MAE is more stable. However, RMSE and MAE are more accurate evaluation metrics compared to other metrics [57]. The equation’s more reliable performance is guaranteed by a condition where MAE and RMSE values are close to 0. Nevertheless, the large variance between RMSE and MAE values represents significant variations in error distribution. Consequently, Mean Relative Error (MRE) was used to measure the precision of the equations applied.

Table 9.Assessment of best alternative equations with different validation metrics for hardness calculation.

Validation Metric Linear Cross-Validation Regression

Linear Cross-Validation with Multiple Regression of Viscosity

Multiple Regression

Equation Based on Biases and Weights

Mean Error 0.0000 0.0000 0.0002 0.0306

Mean Absolute Error 4.8183 3.6826 2.7811 1.8954

Mean Square Error 40.9419 29.2784 22.0436 20.2431

Root Mean Square Error 6.3986 5.4110 4.6951 4.4992

Mean Relative Error 0.0963 0.0727 0.0555 0.0367

Standard Deviation,σ 6.5955 5.5775 4.8396 4.6376

Standard Error of Mean 1.5996 1.3527 1.1738 1.1248

As can be seen in Table9, the suggested Equation Based on Biases and Weight shows much greater reliability compared to other equations, and the next most reliable equation is the Multiple Regression equation. Consequently, both could be applied to precisely calculate the hardness of the SPIF component. Figure 10 illustrates the ability of the developed equations to precisely calculate the hardness of SPIF components compared to the real values of hardness. The fluctuating and uneven hardness in Figure10is normal because the values are for different components formed in various conditions using SPIF.

All of the hardness data were used in predictions models; by sorting these data from low to high or vice versa will affect the random selection of data as training and testing values, which may make it challenging to distinguish the difference between the actual values of hardness and the predicted values by various models in the figure. The HV of points 1–4 is related to the feed rate, 5–8 is related to the spindle speed, 9–12 is related to the tool diameter, and the rest is related to the four types of grease and one coolant oil.

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